反应条件
1: 1) NaH / 1) toluene, reflux, 30 min, 2) reflux, 1 h
2: 51.4 percent / NaBH4 / ethanol / 6 h
4: NaBH4 / methanol / Ambient temperature
5: toluene-p-sulfonic acid / toluene / 4 h / Heating
6: 96 percent / diisobutylaluminium hydride / diethyl ether; hexane / 1) -78 deg C to room temperature, 2) room temperature, 8 h
7: 91.3 percent / N-bromosuccinimide, Me2S / CH2Cl2 / 1) -30 deg C, 3 h, 2) room temperature, 1 h
8: 44.7 percent / m-chloroperbenzoic acid / CH2Cl2 / 1) 0 deg C, 1 h, 2) room temperature, 12 h
9: 33 percent / Bu3SnH, azoisobutyronitrile / benzene / 15 h / Heating
View Scheme
参考文献
Murphy, John A.; Patterson, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 4 p. 405 - 410
