反应条件
1: 1) LDA / 1) THF, hexane, -78 deg C, 10 min, 2) a) -78 deg C, 2 h, b) -20 deg C, 2 h, c) to r.t., 2 h
2: 82 percent / H2 / Pd/C / ethanol / 4 h
3: 92 percent / LiAlH4 / diethyl ether / 2 h / 0 °C
View Scheme
参考文献
Takeda, Momotaro; Takatsu, Keishi; Shintani, Ryo; Hayashi, Tamio
Journal of Organic Chemistry, 2014 , vol. 79, # 6 p. 2354 - 2367
