反应条件
1: 1.) Mg, I2 / 1.) ether, reflux, 1 h, 2.) ether, reflux, 4h; benzene, reflux, overnight
2: 96 percent / LiAlH4 / diethyl ether / 3 h / Heating
3: 81 percent / pyridine / 4 h / 0 °C
4: 82 percent / KI / H2O; dimethylformamide / 4.5 h / 90 °C
5: 82 percent / aq. KOH / ethane-1,2-diol / 5 h / Heating
View Scheme
参考文献
Cheung, Julie; Field, Leslie D.; Regaglia, Francesca; Sternhell, Sever
Australian Journal of Chemistry, 1995 , vol. 48, # 10 p. 1707 - 1726
