5-(4-硝基苯基)呋喃-2-羧酸甲酯合成路线 (共 4 条)
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; P=2280 Torr; 2 h;
参考文献
Lee, Sunkyung; Yi, Kyu Yang; Hwang, Sun Kyung; Lee, Byung Ho; Yoo, Sung-Eun; Lee, Kyunghee
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2882 - 2891
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl acetamide
T=130°C; 20 h; Inert atmosphere; regioselective reaction;
参考文献
Fu, Hai Yan; Doucet, Henri
European Journal of Organic Chemistry, 2011 , # 35 p. 7163 - 7173
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in methanol; toluene
Suzuki reaction; 6 h; Heating;
参考文献
Lee, Sunkyung; Yi, Kyu Yang; Hwang, Sun Kyung; Lee, Byung Ho; Yoo, Sung-Eun; Lee, Kyunghee
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2882 - 2891
反应条件
triethylamine
2.5 h;
参考文献
SPIROGEN LIMITED
Patent: WO2005/85177 A2, 2005 ;
Location in patent: Page/Page column 44-45 ;