2-(苯基磺酰基-甲基)-环氧乙烷合成路线 (共 26 条)
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in 1,4-dioxane T=90°C; 2 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 2 p. 667 - 672
参考文献
Freiter,E.R. et al.
Journal of Medicinal Chemistry, 1973 , vol. 16, # 5 p. 510 - 512
反应条件
1: 92 percent / PdCl2(MeCN)2, CuCl2, air / CH2Cl2 / 16 h / Ambient temperature; Irradiation 2: pyridine View Scheme
参考文献
Muzart, Jacques; Riahi, Abdelkhalek
Journal of Organometallic Chemistry, 1992 , vol. 433, # 3 p. 323 - 336
反应条件
T=100°C; 0.25 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kalugin, V. E.; Litvinov, V. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 7 p. 1391 - 1394
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 7 p. 1574 - 1578
反应条件
1: 1, NaH / 1) THF 2: NiCl2(dppp) / toluene / 3 h / 0 °C View Scheme
参考文献
Sugimura, Hideyuki; Takei, Hisashi
Chemistry Letters, 1984 , p. 1505 - 1508
反应条件
potassium chloride; ammonium chloride in methanol; water T=70°C;
参考文献
Wielechowska, Monika; Plenkiewicz, Jan
Tetrahedron Asymmetry, 2005 , vol. 16, # 6 p. 1199 - 1205
反应条件
sodium hydroxide in 1,4-dioxane
4 h; Ambient temperature;
参考文献
Gu, Xue-Ping; Ikeda, Isao; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 667 - 672
反应条件
sodium hydroxide; sodium chloride in 1,4-dioxane; water
参考文献
Sankyo Company, Limited
Patent: US5578620 A1, 1996 ;
参考文献
Apparao, Satyam; Schmidt, Richard R.
Synthesis, 1987 , # 10 p. 896 - 899
反应条件
potassium carbonate in methanol
3 h; Ambient temperature; Yield given;
参考文献
Yoon, Nung Min; Choi, Jaesung; Ahn, Jin Hee
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3490 - 3493