2-(苯基磺酰基-甲基)-环氧乙烷合成路线 （共 26 条）
反应条件
1: 95 percent Chromat. / borohydride exchange resin / methanol / 3 h / Ambient temperature
2: aq. K2CO3 / methanol / 3 h / Ambient temperature
View Scheme
参考文献
Yoon, Nung Min; Choi, Jaesung; Ahn, Jin Hee
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3490 - 3493
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in 1,4-dioxane
T=100°C; 2 h;
参考文献
Gu, Xue-Ping; Ikeda, Isao; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 667 - 672
反应条件
sodium hydroxide; cyclohexyl monochloride; tetra(n-butyl)ammonium hydrogensulfate in 1,4-dioxane
T=100°C; 2 h;
参考文献
Gu, Xue-Ping; Ikeda, Isao; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 667 - 672
反应条件
2: 57 percent / 30percent H2O2 / CH2Cl2 / 0.25 h / Ambient temperature
View Scheme
参考文献
Figueredo, Marta; Font, Josep; Virgili, Albert
Tetrahedron, 1987 , vol. 43, # 8 p. 1881 - 1886
参考文献
Sheng, Shou-Ri; Huang, Pei-Gang; Zhou, Wei; Luo, Hai-Rong; Lin, Shu-Ying; Liu, Xiao-Ling
Synlett, 2004 , # 14 p. 2603 - 2605
反应条件
1: 1N sulfuric acid / 1 h / Ambient temperature
2: NaIO4 / 1 h / Ambient temperature
View Scheme
参考文献
Ohta, Hiromichi; Miyamae, Yoshitaka; Tsuchihashi, Gen-ichi
Agricultural and Biological Chemistry, 1989 , vol. 53, # 1 p. 215 - 222
参考文献
Pollard; Christie
Journal of Organic Chemistry, 1958 , vol. 23, p. 1333
反应条件
TNM in dichloromethane
Irradiation;
参考文献
Ramkumar; Sankararaman
Synthesis, 1993 , # 11 p. 1057 - 1058
反应条件
in tetrahydrofuran; water
48 h;
参考文献
Apparao, Satyam; Schmidt, Richard R.
Synthesis, 1987 , # 10 p. 896 - 899
反应条件
1: 1, NaH / 1) THF
2: 95 percent / NiCl2(dppp) / benzene / 2.5 h / Ambient temperature; var. Reag.: NiCl2(PPh3)2, 18 h
View Scheme
参考文献
Sugimura, Hideyuki; Takei, Hisashi
Chemistry Letters, 1984 , p. 1505 - 1508
