(2,4-二羟基苯基)(4-甲氧基苯基)甲酮合成路线 (共 6 条)
反应条件
1: methoxybenzene With polymer-supported phenyliodine(III) diacetate; sulfuric acid in acetic acid
T=20°C; Substitution; 20 h;
2: 2,4-dihydroxy-benzaldehyde With sodium carbonate; lithium chloride; palladium dichloride in N,N-dimethyl-formamide
T=60 - 70°C; Substitution; 6 h;
参考文献
Chen
Synlett, 2000 , # 8 p. 1175 - 1177
反应条件
sodium carbonate; lithium chloride; palladium dichloride in N,N-dimethyl-formamide
T=60°C; Arylation; 4 h;
参考文献
Xia, Min; Chen, ZhenChu
Synthetic Communications, 2000 , vol. 30, # 3 p. 531 - 536
反应条件
hydrogen fluoride
T=100°C; unter Druck;
参考文献
VanAllan; Tinker
Journal of Organic Chemistry, 1954 , vol. l9, p. 1243,1244
反应条件
aluminium trichloride; nitrobenzene
参考文献
Johnson; Robertson
Journal of the Chemical Society, 1950 , p. 2381,2386
反应条件
potassium carbonate in acetone
20 h; Heating;
参考文献
Beger, J.; Binte, H.-J.; Brunne, L.; Neumann, R.
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1992 , vol. 334, # 3 p. 269 - 277
反应条件
potassium carbonate; acetone
参考文献
Johnson; Robertson
Journal of the Chemical Society, 1950 , p. 2381,2386