4,4’-(1,3-丙二氧基)二苯胺合成路线 （共 12 条）
反应条件
5 platinum on carbon; hydrazine hydrate in ethanol 18 h; Reflux;
参考文献
Khalid, Naila; Khan, Muhammad Saif Ullah; Siddiqi, Humaira Masood; Akhter, Zareen; Iqbal, Naseer
Journal of the Chemical Society of Pakistan, 2011 , vol. 33, # 4 p. 570 - 577
反应条件
hydrogenchloride; sodium hydroxide in water
参考文献
The Dow Chemical Company
Patent: US4683333 A1, 1987 ;
反应条件
1: 80 percent / K2CO3; KI / acetonitrile / 48 h / Heating 2: 80 percent / H2 / Pd/C / methanol / 40 °C View Scheme
参考文献
Tetrahedron, , vol. 61, # 22 p. 5351 - 5362
反应条件
1: With hydrogenchloride in ethanol; water 6 h; Reflux; 2: With sodium hydroxide in ethanol; water Cooling with ice;
参考文献
Katritzky, Alan R.; Girgis, Adel S.; Slavov, Svetoslav; Tala, Srinivasa R.; Stoyanova-Slavova, Iva
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 11 p. 5183 - 5199
反应条件
1: dimethylformamide / 10 h / Heating 2: H2 / 5percent Pd/C / tetrahydrofuran; methanol / 2280 Torr View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 28, # 11 p. 1728 - 1740
反应条件
1: ethylene glycol 2: Raney nickel; ethyl acetate / 60 °C / 26600 Torr / Hydrogenation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 74, p. 5229
反应条件
sodium hydrogencarbonate in water 1 h;
参考文献
Molecular crystals and liquid crystals, , vol. 105, # 1-4 p. 305 - 314
反应条件
1: anhydrous K2CO3 / dimethylformamide / 4 h / Heating 2: HCl / ethanol 3: NaHCO3 / H2O / 1 h View Scheme
参考文献
Molecular crystals and liquid crystals, , vol. 105, # 1-4 p. 305 - 314
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 130 °C 2: 5 platinum on carbon; hydrazine hydrate / ethanol / 18 h / Reflux View Scheme
参考文献
Journal of the Chemical Society of Pakistan, , vol. 33, # 4 p. 570 - 577
参考文献
Journal of the Chemical Society, , p. 390,391
