4’-甲氧基联苯-4-甲醛合成路线 （共 36 条）
反应条件
1: triphenylphosphine; AcOK / PdCl2(PPh3)2 / toluene / Heating 2: Na2CO3; Bu4NHSO4 / Pd(PPh3)4 / H2O; toluene / Heating View Scheme
参考文献
Synthetic Communications, , vol. 37, # 5 p. 667 - 674
反应条件
1: triphenylphosphine; AcOK / PdCl2(PPh3)2 / toluene / Heating 2: Na2CO3; Bu4NHSO4 / Pd(PPh3)4 / Heating View Scheme
参考文献
Synthetic Communications, , vol. 37, # 5 p. 667 - 674
反应条件
1: NBS 2: NaOEt, iPrNO2 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 96, # 14 p. 4611 - 4616
反应条件
tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; toluene Suzuki cross-coupling; Heating;
参考文献
Synthetic Communications, , vol. 37, # 5 p. 667 - 674
反应条件
1.1: magnesium / tetrahydrofuran / 0.33 h / 80 °C / microwave irradiation 2.1: ZnCl2; TMEDA / tetrahydrofuran / 0.25 h / 80 °C / microwave irradiation 2.2: 81 percent / Pd(PPh3)2Cl2 / tetrahydrofuran / 0.08 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 61, # 47 p. 11168 - 11176
反应条件
1.1: magnesium; 1,2-dibromoethane / tetrahydrofuran / 0.25 h / 180 °C / microwave irradiation 2.1: ZnCl2; TMEDA / tetrahydrofuran / 0.25 h / 80 °C / microwave irradiation 2.2: 87 percent / Pd(PPh3)2Cl2 / tetrahydrofuran / 0.08 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 61, # 47 p. 11168 - 11176
反应条件
NiCl2(PCy3)2 in benzene T=25°C; 2 h;
参考文献
Organometallics, , vol. 30, # 6 p. 1299 - 1302
反应条件
NiCl2(PCy3)2 in benzene T=25°C; 2 h;
参考文献
Organometallics, , vol. 30, # 6 p. 1299 - 1302
反应条件
1: 95 percent / NaOBr 2: 89 percent / diborane 3: 85 percent / Pb(OAc)4/Py View Scheme
参考文献
Analytical Chemistry, , vol. 52, # 14 p. 2417 - 2420
反应条件
1: 69 percent 2: 36 percent / Friedel-Crafts acylation 3: 95 percent / NaOBr 4: 89 percent / diborane 5: 85 percent / Pb(OAc)4/Py View Scheme
参考文献
Analytical Chemistry, , vol. 52, # 14 p. 2417 - 2420
