1.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
2.1: lithium hydroxide hydrate; water / tetrahydrofuran; methanol / 10 h / 20 °C
2.2: pH 2
View Scheme
参考文献
Harvey, James S.; Simonovich, Scott P.; Jamison, Christopher R.; MacMillan, David W. C.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 13782 - 13785