反应条件
1.1: sec.-butyllithium; N,N,N',N,-tetramethylethylenediamine / tetrahydrofuran; cyclohexane / 1 h / -78 °C / |Inert atmosphere 1.2: 1 h / -78 - 20 °C / |Inert atmosphere 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 22 h / 0 °C / |Reflux; |Inert atmosphere 3.1: 5.5 h / 204 °C / |Inert atmosphere 4.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C View Scheme
参考文献
Synthesis (Germany), , vol. 44, # 24 art. no. SS-2012-Z0646-OP, p. 3822 - 3828
