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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
雌酚酮
合成路线
（共 264 条）
84882-50-8
→
反应条件
53-16-7
雌酚酮
+
84882-49-5
反应条件
sulfuric acid in water; acetone 72 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 11 p. 2611 - 2616
566943-59-7
→
反应条件
53-16-7
雌酚酮
反应条件
1.1: 93 percent / TMS-OTf / CH2Cl2 / -78 - 0 °C 2.1: 98 percent / LiAlH4 / tetrahydrofuran 3.1: pyridinium chlorochromate / CH2Cl2 4.1: tetrahydrofuran / -78 °C 5.1: 93 percent / NaH / tetrahydrofuran 6.1: 86 percent / BuSnH; 2,2'-azobisisobutyronitrile / toluene / Heating 7.1: 98 percent / m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 8.1: 64 percent / diisobutylaluminum hydride / CH2Cl2 / -78 °C 9.1: 84 percent / pyridinium chlorochromate / CH2Cl2 10.1: p-TsOH; HOCH2CH2OH / toluene / Heating 10.2: p-TsOH; H2O / acetone / Heating 10.3: Et3SiH; CF3CO2H / benzene 11.1: 84 percent / BBr3 / CH2Cl2 / -30 - 0 °C View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 51, # 1 p. 104 - 106
566943-61-1
→
反应条件
53-16-7
雌酚酮
反应条件
1.1: pyridinium chlorochromate / CH2Cl2 2.1: tetrahydrofuran / -78 °C 3.1: 93 percent / NaH / tetrahydrofuran 4.1: 86 percent / BuSnH; 2,2'-azobisisobutyronitrile / toluene / Heating 5.1: 98 percent / m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 6.1: 64 percent / diisobutylaluminum hydride / CH2Cl2 / -78 °C 7.1: 84 percent / pyridinium chlorochromate / CH2Cl2 8.1: p-TsOH; HOCH2CH2OH / toluene / Heating 8.2: p-TsOH; H2O / acetone / Heating 8.3: Et3SiH; CF3CO2H / benzene 9.1: 84 percent / BBr3 / CH2Cl2 / -30 - 0 °C View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 51, # 1 p. 104 - 106
566943-60-0
→
反应条件
53-16-7
雌酚酮
反应条件
1.1: 98 percent / LiAlH4 / tetrahydrofuran 2.1: pyridinium chlorochromate / CH2Cl2 3.1: tetrahydrofuran / -78 °C 4.1: 93 percent / NaH / tetrahydrofuran 5.1: 86 percent / BuSnH; 2,2'-azobisisobutyronitrile / toluene / Heating 6.1: 98 percent / m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 7.1: 64 percent / diisobutylaluminum hydride / CH2Cl2 / -78 °C 8.1: 84 percent / pyridinium chlorochromate / CH2Cl2 9.1: p-TsOH; HOCH2CH2OH / toluene / Heating 9.2: p-TsOH; H2O / acetone / Heating 9.3: Et3SiH; CF3CO2H / benzene 10.1: 84 percent / BBr3 / CH2Cl2 / -30 - 0 °C View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 51, # 1 p. 104 - 106
566943-64-4
→
反应条件
53-16-7
雌酚酮
反应条件
1.1: 98 percent / m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 2.1: 64 percent / diisobutylaluminum hydride / CH2Cl2 / -78 °C 3.1: 84 percent / pyridinium chlorochromate / CH2Cl2 4.1: p-TsOH; HOCH2CH2OH / toluene / Heating 4.2: p-TsOH; H2O / acetone / Heating 4.3: Et3SiH; CF3CO2H / benzene 5.1: 84 percent / BBr3 / CH2Cl2 / -30 - 0 °C View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 51, # 1 p. 104 - 106
566943-62-2
→
反应条件
53-16-7
雌酚酮
反应条件
1.1: 93 percent / NaH / tetrahydrofuran 2.1: 86 percent / BuSnH; 2,2'-azobisisobutyronitrile / toluene / Heating 3.1: 98 percent / m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 4.1: 64 percent / diisobutylaluminum hydride / CH2Cl2 / -78 °C 5.1: 84 percent / pyridinium chlorochromate / CH2Cl2 6.1: p-TsOH; HOCH2CH2OH / toluene / Heating 6.2: p-TsOH; H2O / acetone / Heating 6.3: Et3SiH; CF3CO2H / benzene 7.1: 84 percent / BBr3 / CH2Cl2 / -30 - 0 °C View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 51, # 1 p. 104 - 106
566943-65-5
→
反应条件
53-16-7
雌酚酮
反应条件
1.1: 64 percent / diisobutylaluminum hydride / CH2Cl2 / -78 °C 2.1: 84 percent / pyridinium chlorochromate / CH2Cl2 3.1: p-TsOH; HOCH2CH2OH / toluene / Heating 3.2: p-TsOH; H2O / acetone / Heating 3.3: Et3SiH; CF3CO2H / benzene 4.1: 84 percent / BBr3 / CH2Cl2 / -30 - 0 °C View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 51, # 1 p. 104 - 106
566943-67-7
→
反应条件
53-16-7
雌酚酮
反应条件
1.1: p-TsOH; HOCH2CH2OH / toluene / Heating 1.2: p-TsOH; H2O / acetone / Heating 1.3: Et3SiH; CF3CO2H / benzene 2.1: 84 percent / BBr3 / CH2Cl2 / -30 - 0 °C View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 51, # 1 p. 104 - 106
566943-66-6
→
反应条件
53-16-7
雌酚酮
反应条件
1.1: 84 percent / pyridinium chlorochromate / CH2Cl2 2.1: p-TsOH; HOCH2CH2OH / toluene / Heating 2.2: p-TsOH; H2O / acetone / Heating 2.3: Et3SiH; CF3CO2H / benzene 3.1: 84 percent / BBr3 / CH2Cl2 / -30 - 0 °C View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 51, # 1 p. 104 - 106
566943-63-3
→
反应条件
53-16-7
雌酚酮
反应条件
1.1: 86 percent / BuSnH; 2,2'-azobisisobutyronitrile / toluene / Heating 2.1: 98 percent / m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 3.1: 64 percent / diisobutylaluminum hydride / CH2Cl2 / -78 °C 4.1: 84 percent / pyridinium chlorochromate / CH2Cl2 5.1: p-TsOH; HOCH2CH2OH / toluene / Heating 5.2: p-TsOH; H2O / acetone / Heating 5.3: Et3SiH; CF3CO2H / benzene 6.1: 84 percent / BBr3 / CH2Cl2 / -30 - 0 °C View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 51, # 1 p. 104 - 106
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