5,6-二氯-1-β-D-呋喃核糖基苯并咪唑合成路线 （共 13 条）
反应条件
nickel in ethanol 8 h; Heating;
参考文献
Devivar, Rodrigo V.; Kawashima, Etsuko; Revankar, Ganapathi R.; Breitenbach, Julie M.; Kreske, Edward D.; et al.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 18 p. 2942 - 2949
反应条件
sodium methylate in methanol Yield given;
参考文献
Carbohydrate Research, , vol. 216, # 1 p. 421 - 439
反应条件
1: N,O-bis(trimethylsilyl)acetamide; trimethylsilyl triflate / acetonitrile / 0.08 h / 130 °C / microwave irradiation 2: NH3 / methanol / 16 h / 50 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 1 p. 173 - 179
反应条件
xylene Behandeln des Reaktionsprodukts mit methanol. Natriummethylat;
参考文献
Journal of the American Chemical Society, , vol. 79, p. 1185,1187
反应条件
1: 95 percent / KOH / ethanol; H2O / 3 h / Heating 2: 1.) bis(trimethylsilyl)acetamide, 2.) TMSOTf / 1.) MeCN, 15 min, 2.) MeCN, 50 deg C, 18 h 3: 76 percent / methanol. NH3 / 18 h / Ambient temperature 4: 78 percent / aq. NH3 / acetonitrile / 18 h / Ambient temperature 5: 85 percent / Raney Ni / ethanol / 8 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 37, # 18 p. 2942 - 2949
反应条件
1: 1.) bis(trimethylsilyl)acetamide, 2.) TMSOTf / 1.) MeCN, 15 min, 2.) MeCN, 50 deg C, 18 h 2: 76 percent / methanol. NH3 / 18 h / Ambient temperature 3: 78 percent / aq. NH3 / acetonitrile / 18 h / Ambient temperature 4: 85 percent / Raney Ni / ethanol / 8 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 37, # 18 p. 2942 - 2949
反应条件
1: 78 percent / aq. NH3 / acetonitrile / 18 h / Ambient temperature 2: 85 percent / Raney Ni / ethanol / 8 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 37, # 18 p. 2942 - 2949
反应条件
1: 76 percent / methanol. NH3 / 18 h / Ambient temperature 2: 78 percent / aq. NH3 / acetonitrile / 18 h / Ambient temperature 3: 85 percent / Raney Ni / ethanol / 8 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 37, # 18 p. 2942 - 2949
反应条件
1: N,O-bis(trimethylsilyl)acetamide; trimethylsilyl triflate / acetonitrile / 0.08 h / 130 °C / microwave irradiation 2: NH3 / methanol / 16 h / 50 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 1 p. 173 - 179
反应条件
sodium methylate in methanol Yield given;
参考文献
Carbohydrate Research, , vol. 216, # 1 p. 421 - 439
