1: 1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indole-3-acetic acid With oxalyl dichloride in dichloromethane T=20°C; 2 h; 2: ethanol With triethylamine in dichloromethane 0.5 h;
anhydrous tetramethylammonium chloride in ethanol electrolysis at a controlled potential; mercury working electrode; graphite as the auxiliary electrode;
参考文献
Boneva, A. S.; Loginova, N. F.; Filippova, T. M.; Mishchenko, V. V.; Bekker, A. R.; et al.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 12 p. 863 - 871
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 12 p. 1494 - 1502
anhydrous tetramethylammonium chloride in ethanol electrolysis at a controlled potential, pH 5.0; mercury working electrode; graphite as the auxiliary electrode;
参考文献
Boneva, A. S.; Loginova, N. F.; Filippova, T. M.; Mishchenko, V. V.; Bekker, A. R.; et al.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 12 p. 863 - 871
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 12 p. 1494 - 1502