烯丙基(乙基)氨基甲酸叔丁酯合成路线 （共 2 条）
反应条件
1: 3-t-butoxycarbonylamino-1-propene With sodium hydride in tetrahydrofuran
T=0 - 20°C; Inert atmosphere;
2: ethyl iodide in tetrahydrofuran
T=0 - 20°C; Inert atmosphere;
参考文献
McMills, Mark C.; Humes, Ross J.; Pavlyuk, Oksana M.
Tetrahedron Letters, 2012 , vol. 53, # 7 p. 849 - 851
反应条件
1: 3-t-butoxycarbonylamino-1-propene With sodium hydride in tetrahydrofuran; DMF (N,N-dimethyl-formamide)
T=40°C;
2: ethyl iodide in tetrahydrofuran; DMF (N,N-dimethyl-formamide)
T=0°C; 16 h;
参考文献
NOVARTIS AG; NOVARTIS PHARMA GMBH
Patent: WO2005/49585 A1, 2005 ;
Location in patent: Page/Page column 408 ;
