4-甲氧基-4-甲基-联苯合成路线 (共 207 条)
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 3-butyl-1-methyl-5-[9-(3-methyl-1H-imidazol-3-ium-1-yl)nonyl]-3H-1,2,3-triazol-1-ium diiodide; caesium carbonate in 1,4-dioxane Suzuki-Miyaura reaction; Inert atmosphereHeating;
参考文献
Synthesis, , # 15 art. no. T02910SS, p. 2609 - 2615
反应条件
potassium carbonate; [PS-PEG-adppp-Pd(η3-C3H5)]Cl in water T=50°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Organic Letters, , vol. 4, # 17 p. 2997 - 3000
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura coupling; 8 h;
参考文献
Journal of the American Chemical Society, , vol. 126, # 10 p. 3058 - 3059
反应条件
sodium hydroxide; PEG encapsulated palladium nanoparticle in water T=90°C; Hiyama cross-coupling reaction; 3.5 h;
参考文献
Organic Letters, , vol. 9, # 18 p. 3639 - 3642
反应条件
tripotassium phosphate monohydrate; 4-bromo-benzoic acid ethyl ester; C52H49PRu; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane T=100°C; Suzuki-Miyaura Coupling; 3 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 78, # 22 p. 11513 - 11524
反应条件
1: 4-methyl-chlorobenzene With HASPO; Ni(acac)2 in tetrahydrofuran T=20°C; 0.0833333 h; 2: 4-methoxyphenyl magnesium bromide in tetrahydrofuran T=20°C; Kumada cross-coupling; 4 h;
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 44 p. 7216 - 7219
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tert.-butylnitrite; trifuran-2-yl-phosphane; acetic acid in N,N-dimethyl-formamide T=90°C; 8 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 52, # 4 p. 518 - 522
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 3-butyl-1-methyl-5-[9-(3-methyl-1H-imidazol-3-ium-1-yl)nonyl]-3H-1,2,3-triazol-1-ium diiodide; caesium carbonate in 1,4-dioxane Suzuki-Miyaura reaction; Inert atmosphereHeating;
参考文献
Synthesis, , # 15 art. no. T02910SS, p. 2609 - 2615
反应条件
potassium carbonate in ethanol; water T=70°C; Suzuki coupling; 1 h; Under air;
参考文献
Tetrahedron Letters, , vol. 52, # 13 p. 1477 - 1480
反应条件
Pd2Cl2(micro;-Cl)2(PPh3)2; potassium carbonate in 1,4-dioxane T=100°C; 4 h; Inert atmosphere;
参考文献
Journal of Organometallic Chemistry, , vol. 698, p. 15 - 21