4-甲氧基-4-甲基-联苯合成路线 (共 207 条)
反应条件
Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=90°C; Negishi coupling reaction; 8 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 21 p. 4901 - 4904
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in toluene Suzuki-Miyaura reaction; 24 h; Heating;
参考文献
Organic Letters, , vol. 8, # 18 p. 4071 - 4074
反应条件
tetrabutyl ammonium fluoride; tris-(o-tolyl)phosphine; dichloro bis(acetonitrile) palladium(II) T=80°C; Hiyama cross-coupling reaction; 1 h;
参考文献
Synthesis, , # 6 p. 969 - 974
反应条件
polystyrene-supported N-heterocyclic carbene-Pd complex in ethanol T=20°C; Suzuki-Miyaura cross-coupling; 10 h;
参考文献
Synlett, , # 15 p. 2410 - 2414
反应条件
bis-triphenylphosphine-palladium(II) chloride; cesium fluoride in N,N-dimethyl-formamide T=80°C; Suzuki-Miyaura cross-coupling; 2 h; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 27 p. 4690 - 4696
反应条件
potassium acetate; palladium diacetate; N,N-dicyclohexylamine in N,N-dimethyl-formamide T=35°C; 2 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 51, # 47 p. 6101 - 6104
反应条件
palladium 10 on activated carbon; tetrabutyl ammonium fluoride; water; tris(p-fluoro phenyl)phosphine in toluene T=120°C; Hiyama coupling; 12 h; Inert atmosphere;
参考文献
Chemistry Letters, , vol. 40, # 9 p. 910 - 912
反应条件
triphenyl-arsane; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in various solvent(s) T=80°C; 70 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 20 p. 5434 - 5444
反应条件
tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethylene glycol dimethyl ether; hexane T=20°C;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1689 - 1692