4-甲氧基-4-甲基-联苯合成路线 （共 207 条）
反应条件
1: p-anisylgermanium trichloride With ammonium hydroxide T=20°C; 2: para-bromotoluene With sodium hydroxide; palladium diacetate in 1,4-dioxane; water 8 h; Heating; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 7 p. 1025 - 1027
反应条件
1: (4-methylphenyl)trichlorogermane With ammonium hydroxide T=20°C; 1 h; 2: para-iodoanisole With sodium hydroxide; P[2,4,6-(OMe)3C6H2]3; palladium diacetate in 1,4-dioxane; water 24 h; Heating; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 7 p. 1025 - 1027
反应条件
1: (4-methylphenyl)trichlorogermane With ammonium hydroxide T=20°C; 1 h; 2: 1-bromo-4-methoxy-benzene With sodium hydroxide; palladium diacetate in 1,4-dioxane; water 8 h; Heating; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 7 p. 1025 - 1027
反应条件
1: p-anisylgermanium trichloride With ammonium hydroxide T=20°C; 2: 1-(iodo)-4-methylbenzene With sodium hydroxide; palladium diacetate in 1,4-dioxane; water 4 h; Heating; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 7 p. 1025 - 1027
反应条件
bis(η3-allyl-μ-chloropalladium(II)); P(C6H4)CH(C(CH3)C(Si(CH3)3))2 in tetrahydrofuran; acetonitrile T=20°C; Negishi coupling reaction; 2 h;
参考文献
Chemistry - A European Journal, , vol. 17, # 51 p. 14389 - 14393
反应条件
tetrabutylammomium bromide; palladium diacetate in water T=20°C; Suzuki-Miyaura coupling; 7 h;
参考文献
Green Chemistry, , vol. 12, # 10 p. 1734 - 1738
反应条件
anhydrous dipotassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki-Miyaura coupling reaction; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 2-3 p. 309 - 314
反应条件
1: para-iodoanisole With [PdCl2(1,3-bis(diphenylphosphino)propane)]; tBuCH2CH2B(H)NiPr2; triethylamine; potassium iodide in toluene T=110°C; Suzuki coupling; 1 h; Inert atmosphere; 2: 1-(iodo)-4-methylbenzene With caesium carbonate in ethanol; water; toluene T=90°C; Suzuki coupling; 15 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 48, # 10 p. 1553 - 1555
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 2 p. 1018 - 1025
反应条件
SPHOS; tris-(dibenzylideneacetone)dipalladium(0); nonafluoro-n-butanesulfonyl fluoride; caesium carbonate in acetonitrile T=60°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Synlett, , vol. 23, # 15 p. 2241 - 2246
