4-甲氧基-4-甲基-联苯合成路线 (共 207 条)
反应条件
potassium phosphate; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in toluene T=110°C; Suzuki-Miyaura Coupling; 24 h; Schlenk technique;
参考文献
Journal of Organic Chemistry, , vol. 78, # 10 p. 5078 - 5084
反应条件
potassium phosphate; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in toluene T=110°C; Suzuki-Miyaura Coupling; 24 h; Schlenk technique;
参考文献
Journal of Organic Chemistry, , vol. 78, # 10 p. 5078 - 5084
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium hydroxide in neat (no solvent) T=110°C; Suzuki-Miyaura Coupling; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 18 p. 3553 - 3557
反应条件
tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethylene glycol dimethyl ether; hexane T=20°C; 18 h; Product distribution; Further Variations:CatalystsReagents;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1689 - 1692
反应条件
N2 in dichloromethane; ethyl acetate; N,N-dimethyl-formamide
反应条件
palladium diacetate; silver carbonate; di-tert-butyl(2′,4′,6′-triisopropylbiphenyl-2-yl)phosphine in dimethyl sulfoxide; N,N-dimethyl-formamide T=200°C; 0.0833333 h; MicrowaveMolecular sieve;
参考文献
Chemical Communications, , # 47 p. 6312 - 6314
反应条件
1,3-bis-(diphenylphosphino)propane; potassium carbonate; nickel dichloride in 1,4-dioxane T=100°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 16, # 17 p. 4991 - 4994
反应条件
C68H72Cl2N6NiP2 in diethyl ether T=25°C; Kumada coupling reaction; 12 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 16, # 34 p. 10332 - 10336
反应条件
C68H72Cl2N6NiP2 in diethyl ether T=25°C; Kumada coupling reaction; 12 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 16, # 34 p. 10332 - 10336
反应条件
potassium phosphate; Ni(PCy3)2Cl2 in toluene T=180°C; Suzuki-Miyaura cross-coupling; 0.166667 h; Microwave irradiationInert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 76, # 5 p. 1507 - 1510