4-甲氧基-4-甲基-联苯合成路线 (共 207 条)
反应条件
potassium phosphate; Ni(PCy3)2Cl2 in 1,4-dioxane T=110°C; Suzuki-Miyaura coupling; 24 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 76, # 7 p. 2338 - 2344
反应条件
[NiCl2(PMe3)2] in tetrahydrofuran T=70°C; 12 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 9 p. 1641 - 1645
反应条件
1: With n-hexylMgCl; FeBr2; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; 0.0833333 h; Inert atmosphere; 2: in di-isopropyl ether; toluene T=120°C; 48 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 134, # 36 p. 14638 - 14641
反应条件
caesium carbonate; palladium dichloride in N,N-dimethyl-formamide T=185°C; 20 h; Inert atmosphereSealed tube;
参考文献
Synlett, , vol. 24, # 13 art. no. ST-2013-S0280-L, p. 1715 - 1721
反应条件
C39H32OP2*CuCl; sodium t-butanolate in toluene T=80°C; Suzuki-Miyaura Coupling; 15 h; Inert atmosphereGlovebox;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 13 p. 3475 - 3479
Angew. Chem., , vol. 126, # 13 p. 3543 - 3547,5
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran 28 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 68, # 8 p. 3017 - 3025
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran; diethyl ether 12 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 70, # 4 p. 1482 - 1485
反应条件
1: 1-bromo-4-methoxy-benzene With magnesium in tetrahydrofuran 2: With zinc dibromide in tetrahydrofuran 3: para-bromotoluene With bis(acetylacetonate)nickel(II) in tetrahydrofuran T=25°C; Negishi cross-coupling; 6 h;
参考文献
Tetrahedron, , vol. 62, # 32 p. 7521 - 7533
反应条件
potassium carbonate in N,N-dimethyl acetamide; water T=100°C; Suzuki-Miyaura coupling; 48 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 14-15 p. 2823 - 2836
反应条件
bis(η3-allyl-μ-chloropalladium(II)); tri-tert-butyl phosphine; potassium hydroxide in water; toluene; tert-butyl alcohol T=80°C;
参考文献
Chemistry - A European Journal, , vol. 17, # 47 p. 13230 - 13239