4-甲氧基-4-甲基-联苯合成路线 (共 207 条)
反应条件
C27H22Cl2N3NiP in tetrahydrofuran; 1-methyl-pyrrolidin-2-one 12 h; Inert atmosphereSchlenk techniqueHeating;
参考文献
Dalton Transactions, , vol. 41, # 34 p. 10453 - 10464,12
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; phosphate potassium salt in 1,1-dimethylpropan-1-ol T=80°C; P=413.729 Torr; 12 h;
参考文献
Organic Letters, , vol. 15, # 19 p. 5008 - 5011
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran 28 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 68, # 8 p. 3017 - 3025
反应条件
1.1: n-BuLi / hexane / 1 h / 20 °C 1.2: 81 percent / hexane / 1 h / -78 °C 2.1: 88 percent / NaOH / PEG encapsulated palladium nanoparticle / H2O / 3.5 h / 90 °C View Scheme
参考文献
Organic Letters, , vol. 9, # 18 p. 3639 - 3642
反应条件
copper(l) iodide; cesium fluoride in N,N-dimethyl-formamide T=20°C; Stille coupling; 12 h; Inert atmosphere;
参考文献
New Journal of Chemistry, , vol. 35, # 12 p. 2740 - 2742
反应条件
1.1: 73 percent / diethyl ether / 0 - 20 °C 2.1: TBAF / tetrahydrofuran 2.2: 92 percent / TBAF; (t-Bu)3P / [(allyl)PdCl]2 / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Organic Letters, , vol. 1, # 9 p. 1495 - 1498
反应条件
1: 89 percent / pyridine / CHCl3 / 12 h / 20 °C 2: 78 percent / dppfNiCl2 / tetrahydrofuran / 28 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 8 p. 3017 - 3025
反应条件
1-phenyl-3-isopropylimidazolium iodide; palladium diacetate; caesium carbonate in 1,4-dioxane T=80°C; Suzuki-Miyaura coupling; 24 h; Inert atmosphere;
参考文献
Organometallics, , vol. 29, # 23 p. 6343 - 6349
反应条件
C30H21F6N2NiO2P in tetrahydrofuran T=70°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Catalysis Letters, , vol. 143, # 5 p. 424 - 431
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran 28 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 68, # 8 p. 3017 - 3025