4-甲氧基-4-甲基-联苯合成路线 （共 207 条）
反应条件
1.1: sodium nitrite; hydrochloric acid / 0 °C 1.2: 1.99 g / potassium carbonate / H2O; tetrahydrofuran / 0.5 h 2.1: 76 percent / BF3*OEt2 / Pd(OAc)2 / methanol / 3 h / 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 78, # 9 p. 1654 - 1658
反应条件
1-phenyl-3-isopropylimidazolium iodide; palladium diacetate; caesium carbonate in 1,4-dioxane T=80°C; Suzuki-Miyaura coupling; 24 h; Inert atmosphere;
参考文献
Organometallics, , vol. 29, # 23 p. 6343 - 6349
反应条件
potassium carbonate in ethanol; water T=120°C; Suzuki-Miyaura reaction; 2.5 h; continuous flow;
参考文献
Tetrahedron Letters, , vol. 53, # 32 p. 4166 - 4168
反应条件
dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran T=20°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 26, # 39 p. 4819 - 4822
反应条件
tetrabutyl ammonium fluoride; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane 24 h; Heating; Yield given;
参考文献
Synlett, , # 1 p. 63 - 64
反应条件
tetrabutyl ammonium fluoride; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane 24 h; Heating; Yield given;
参考文献
Synlett, , # 1 p. 63 - 64
反应条件
tetrabutyl ammonium fluoride; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane 24 h; Heating; Yield given;
参考文献
Synlett, , # 1 p. 63 - 64
反应条件
1: 100 percent / aq. NaOH / toluene 2: 90 percent / 1,1'-bis(diphenylphosphino)ferrocene dichloropalladium / toluene / 24 h / Heating View Scheme
参考文献
Organic Letters, , vol. 8, # 18 p. 4071 - 4074
反应条件
1.1: sodium nitrite; hydrochloric acid / 0 °C 1.2: potassium carbonate / H2O; tetrahydrofuran 2.1: BF3*OEt2 / Pd(OAc)2 / methanol / 3 h / 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 78, # 9 p. 1654 - 1658
反应条件
1.1: 91 percent / diethyl ether / 12 h / Heating 2.1: tetrabutylammonium fluoride trihydrate / dimethylsulfoxide; H2O / 1 h / 20 °C 2.2: 94 percent / PCy3 / PdCl2 / dimethylsulfoxide; H2O / 6 h / 80 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1715 - 1727
