4-甲氧基-4-甲基-联苯合成路线 (共 207 条)
反应条件
1: 69 percent / diethyl ether 2: 68 percent / silver(I) oxide / [Pd(PPh3)4] / tetrahydrofuran / 7 h / 60 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 73, # 3 p. 749 - 750
反应条件
bis(acetylacetonate)nickel(II) in tetrahydrofuran; diethyl ether 3 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 7 - 14
反应条件
1.1: 7.5 g / diethyl ether / 12 h / Heating 2.1: tetrabutylammonium fluoride trihydrate / tetrahydrofuran; H2O / 1 h / 20 °C 2.2: 95 percent / 2-dicyclohexylphosphino-2',4',6'-triisopropylbiphenyl / [(η3-C3H5)PdCl]2 / tetrahydrofuran; H2O / 4 h / 80 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1715 - 1727
反应条件
phenylnickel N-Bu-6-[1-(2,6-(Me)2PhN)ethyl]picolinamide in tetrahydrofuran; toluene T=80°C; 24 h;
参考文献
Journal of Organometallic Chemistry, , vol. 693, # 8-9 p. 1683 - 1695
反应条件
1: dichloromethane / 4 h / 20 °C / Inert atmosphere 2: Ni(PCy3)2Cl2 / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 8 h / 90 °C / Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 21 p. 4901 - 4904
反应条件
C27H31Br2N5Ni in tetrahydrofuran T=30°C; Tamao-Kumada-Corriu coupling; 24 h; Inert atmosphere;
参考文献
Australian Journal of Chemistry, , vol. 65, # 7 p. 823 - 833
反应条件
palladium diacetate in methanol T=20°C; 14 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 78, # 9 p. 1654 - 1658
反应条件
1: 74 percent / Pd(PPh3)4; Na2CO3 / H2O; toluene; ethanol / 6 h / Heating 2: 80 percent / dppeNiCl2 / tetrahydrofuran; diethyl ether / 12 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 4 p. 1482 - 1485
反应条件
1: 65 percent / H2O; aniline / diethyl ether / 0.33 h / 0 °C 2: 99 percent / Pd(PPh3)4; Ag2O / tetrahydrofuran / 12 h / 60 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 17 p. 5342 - 5349
反应条件
1: 82 percent / NEt3 2: methanol / 1 h / Ambient temperature; Irradiation View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 60, # 1.2 p. 1 - 14