4-甲氧基-4-甲基-联苯合成路线 （共 207 条）
反应条件
[Ni0(1,5-cyclooctadiene)2]; cesium fluoride; tri-cyclo-hexyl-phosphine in toluene T=20 - 100°C; Suzuki-Miyaura coupling; 12 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 133, # 48 p. 19505 - 19511
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride in N,N-dimethyl-formamide T=185°C; 20 h; Inert atmosphere;
参考文献
Synthesis (Germany), , vol. 45, # 5 art. no. SS-2012-M0902-OP, p. 694 - 702
反应条件
C30H21F6N2NiO2P; lithium tert-butylate in tetrahydrofuran T=70°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Catalysis Letters, , vol. 143, # 5 p. 424 - 431
反应条件
copper(l) iodide; cesium fluoride in N,N-dimethyl-formamide T=20°C; Stille coupling; 18 h; Inert atmosphere;
参考文献
New Journal of Chemistry, , vol. 35, # 12 p. 2740 - 2742
反应条件
1.1: tert.-butyl lithium / diethyl ether; pentane / 0.5 h / -78 °C / |Inert atmosphere 1.2: -78 - 0 °C 2.1: tetrahydrofuran / 110 °C / |Inert atmosphere View Scheme
参考文献
European Journal of Organic Chemistry, , # 35 p. 7891 - 7894
反应条件
tris(dibenzylideneacetone)dipalladium (0); sodium carbonate; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride in tetrahydrofuran Suzuki-Miyaura cross-coupling; Heating; Product distribution; Further Variations:Reagents;
参考文献
Organic Letters, , vol. 6, # 1 p. 95 - 98
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; Negishi cross-coupling; 96 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 16, # 1 p. 248 - 253
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; Negishi cross-coupling; 192 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 16, # 1 p. 248 - 253
反应条件
C34H38Cl2N4Pd; caesium carbonate in 1,4-dioxane T=100°C; Suzuki coupling; 25 h;
参考文献
Dalton Transactions, , # 11 p. 2020 - 2028
反应条件
1: 1-bromo-4-methoxy-benzene With magnesium in diethyl ether 2: para-bromotoluene in diethyl ether Kumada coupling reaction; 3 h; Reflux;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 2 p. 331 - 335
