4-甲氧基-4-甲基-联苯合成路线 (共 207 条)
反应条件
NiCl2((PPh3)P)2; (4-Methylphenyl)-magnesium bromide in tetrahydrofuran; diethyl ether 3 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 7 - 14
反应条件
anhydrous iron chloride; lithium hexamethyldisilazane; N-methyl-2-(methylamino)ethylamine T=20 - 80°C; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 11 p. 2004 - 2008
反应条件
water; caesium carbonate; potassium iodide in methanol Suzuki-Miyaura coupling; 12 h; Reflux;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 34 p. 8525 - 8528
反应条件
bathophenanthroline; sodium t-butanolate T=172°C; 12 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 132, # 44 p. 15537 - 15539
反应条件
1: diethyl ether / Erhitzen des nach der Hydrolyse erhaltenen Reaktionsprodukts unter 4 Torr 2: sulfur / 220 - 240 °C View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 26, p. 296,299
反应条件
HCN(CH2C(O)NHC6H5)CHCHN(CH2C6H5)(1+)*Cl(1-)=(HCN(CH2C(O)NHC6H5)CHCHN(CH2C6H5))Cl; potassium tert-butylate T=20 - 100°C; 24 h; Schlenk techniqueInert atmosphereGreen chemistry; Overall yield = 62 percentSpectr.; regioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 356, # 2-3 p. 406 - 410
反应条件
[2,2']bipyridinyl; triphenylphosphine; nickel dichloride; zinc 1.) N,N'-dimethylacetamide, 70 deg C, 1 h, 2.) 70 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 51, # 14 p. 2627 - 2637
参考文献
Journal of the Indian Chemical Society, , vol. 12, p. 690
参考文献
Journal of the Chemical Society [Section] B: Physical Organic, , vol. <B>, p. 779 - 785
反应条件
palladium diacetate in 1,4-dioxane T=20°C; Arylation; 4 h; Product distribution; Further Variations:CatalystsReaction partnersSolventsreaction times;
参考文献
European Journal of Organic Chemistry, , # 8 p. 1875 - 1883