4-甲氧基-4-甲基-联苯合成路线 (共 207 条)
反应条件
potassium phosphate; Ni(COD)2; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 8 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 10, # 21 p. 4879 - 4882
反应条件
1: triallyl(4-methylphenyl)silane With tetrabutyl ammonium fluoride in water; dimethyl sulfoxide T=20°C; 1 h; 2: 1-bromo-4-methoxy-benzene With tri-cyclo-hexyl-phosphine; palladium dichloride in water; dimethyl sulfoxide T=80°C; 6 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1715 - 1727
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C; 0.5 h; 2: para-bromotoluene in tetrahydrofuran T=0 - 25°C; 10 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 348, # 9 p. 1086 - 1092
反应条件
palladium diacetate in water; N,N-dimethyl-formamide T=20°C; 22 h;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 5 p. 928 - 931
反应条件
Ni(Cl){2-(Ph2P)C6H4NCH(Ph)P(O)Ph2} in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=70°C; Negishi coupling reaction; 12 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 5 p. 1598 - 1600
反应条件
Pd0(tris(tert-butyl)phosphine)2 in toluene T=90°C; 3 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 131, # 8 p. 3104 - 3118
反应条件
water; palladium diacetate; sodium carbonate T=80°C; Suzuki Coupling; 4 h; Green chemistry;
参考文献
Green Chemistry, , vol. 16, # 4 p. 2185 - 2189
反应条件
tetrabutyl ammonium fluoride; tris-(o-tolyl)phosphine; dichloro bis(acetonitrile) palladium(II) T=80°C; Hiyama cross-coupling reaction; 0.75 h;
参考文献
Synthesis, , # 6 p. 969 - 974
反应条件
bis(carbene)-derived nickel(II)-pincer complex in tetrahydrofuran T=20°C; Grignard coupling reaction; 48 h;
参考文献
Synthesis, , # 18 p. 2853 - 2861
反应条件
potassium hydroxide; palladium diacetate in methanol T=60°C; Suzuki-Miyaura cross-coupling;
参考文献
Journal of Organic Chemistry, , vol. 72, # 24 p. 9346 - 9349