4-甲氧基-4-甲基-联苯合成路线 (共 207 条)
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium lauryl sulfate; potassium carbonate; p-toluenesulfonyl chloride in water T=60°C; Suzuki Coupling; Catalytic behavior; Reagent/catalystTemperature;
参考文献
Tetrahedron Letters, , vol. 55, # 17 p. 2872 - 2875
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(l) oxide in tetrahydrofuran T=60°C; Arylation; 12 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 17 p. 5342 - 5349
反应条件
triphenyl-phosphine oxide; bis(η3-allyl-μ-chloropalladium(II)) in toluene T=90°C; 0.583333 h;
参考文献
Tetrahedron, , vol. 63, # 26 p. 5730 - 5738
反应条件
1.1: BuLi / diethyl ether; hexane / 1 h / -78 °C 1.2: 63 percent / diethyl ether; hexane / 13 h / 20 °C 2.1: 75 percent / Ag2O / Pd(PPh3)4 / tetrahydrofuran / 36 h / 60 °C View Scheme
参考文献
Organic Letters, , vol. 1, # 2 p. 299 - 301
反应条件
palladium diacetate in nitrogen
反应条件
Pd/Fe3O4; cesium fluoride in 1,4-dioxane T=100°C; Stille Cross Coupling; 18 h;
参考文献
Bulletin of the Korean Chemical Society, , vol. 33, # 8 p. 2789 - 2792
反应条件
bis-triphenylphosphine-palladium(II) chloride; cesium fluoride in N,N-dimethyl-formamide T=80°C; Suzuki-Miyaura cross-coupling; 2 h; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 27 p. 4690 - 4696
反应条件
palladium diacetate; potassium carbonate in butanone T=120°C; Ullmann reaction; 12 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 11, # 5 p. 1079 - 1082
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; ethylene glycol dimethyl ether T=0 - 20°C; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 38, # 25 p. 4397 - 4400
反应条件
caesium carbonate; tri-cyclo-hexyl-phosphine; palladium diacetate in tetrahydrofuran Suzuki-Miyaura reaction; 21 h; Heating;
参考文献
Synlett, , # 11 art. no. Y00205ST, p. 1763 - 1766