4-甲氧基-4-甲基-联苯合成路线 (共 207 条)
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium hydroxide in neat (no solvent) T=110°C; Suzuki-Miyaura Coupling; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 18 p. 3553 - 3557
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
European Journal of Organic Chemistry, , # 21 p. 4884 - 4890
反应条件
1: 4-methoxy-benzoic acid With copper (II) iodide in various solvent(s) T=160°C; 0.5 h; 2: para-bromotoluene With potassium fluoride; palladium acetylacetonate; iso-propyldiphenylphosphine in various solvent(s) T=160°C; 24 h; Further stages.;
参考文献
Journal of the American Chemical Society, , vol. 129, # 15 p. 4824 - 4833
反应条件
sodium carbonate; polystyrene-supported N-heterocyclic carbene-Pd complex in tetrahydrofuran Suzuki cross-coupling; 15 h; Heating;
参考文献
Synlett, , # 12 p. 1891 - 1894
反应条件
sodium carbonate; polystyrene-supported N-heterocyclic carbene-Pd complex in tetrahydrofuran Suzuki cross-coupling; 15 h; Heating;
参考文献
Synlett, , # 12 p. 1891 - 1894
反应条件
caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide T=90°C; 2 h;
参考文献
Tetrahedron, , vol. 64, # 24 p. 5762 - 5772
反应条件
bis-triphenylphosphine-palladium(II) chloride; cesium fluoride in N,N-dimethyl-formamide T=80°C; Suzuki-Miyaura cross-coupling; 2 h; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 27 p. 4690 - 4696
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate in N,N-dimethyl acetamide; water T=60°C; Suzuki-Miyaura cross-coupling;
参考文献
Organic Letters, , vol. 11, # 7 p. 1463 - 1466
反应条件
sodium carbonate; palladium dichloride in methanol T=20°C; Suzuki-Miyaura cross-coupling reaction; 0.333333 h;
参考文献
Tetrahedron, , vol. 66, # 38 p. 7633 - 7641
反应条件
1: p-methylphenylboronic acid With CpPd(IMes)Cl; potassium tert-butylate T=23°C; Inert atmosphere; 2: 1-methoxy-4-chlorobenzene in isopropyl alcohol T=23°C; 2 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 10 p. 1575 - 1585