(4-甲氧基二苯-3-基)胺 1盐酸盐合成路线 （共 8 条）
反应条件
palladium on activated charcoal; hydrazine hydrate in ethanol T=20°C; 2 h;
参考文献
Vangala, Venu R.; Bhogala, Balakrishna R.; Dey, Archan; Desiraju, Gautam R.; Broder, Charlotte K.; Smith, Philip S.; Mondal, Raju; Howard, Judith A. K.; Wilson, Chick C.
Journal of the American Chemical Society, 2003 , vol. 125, # 47 p. 14495 - 14509
反应条件
lithium chloride; Palladacycle in various solvent(s) T=90°C; 5 h;
参考文献
Brody, Marcus S.; Finn
Tetrahedron Letters, 1999 , vol. 40, # 3 p. 415 - 418
反应条件
palladium diacetate; potassium carbonate in tetrahydrofuran; water Suzuki-Miyaura coupling; 12 h; Inert atmosphereReflux;
参考文献
Razler, Thomas M.; Hsiao, Yi; Qian, Feng; Fu, Ruiling; Khan, Rana Kashif; Doubleday, Wendel
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1381 - 1384
反应条件
1: 80 percent / Pd(OAc)2; DAB-Cy; Cs2CO3 / dioxane / 4 h / Heating 2: 70 percent / N2H4*H2O; Pd/C / ethanol / 2 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 47 p. 14495 - 14509
反应条件
1: 80 percent / Pd(OAc)2; DAB-Cy; Cs2CO3 / dioxane / 4 h / Heating 2: 70 percent / N2H4*H2O; Pd/C / ethanol / 2 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 47 p. 14495 - 14509
反应条件
1: triethylamine / dichloromethane / 6 h / 0 - 20 °C 2: palladium diacetate; tricyclopentyl-phosphine; potassium carbonate / toluene / 8 h / 95 °C / |Glovebox View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 37 p. 13664 - 13667
反应条件
1: sodium acetate; hydroxylamine hydrochloride / methanol / 4 h / |Reflux 2: triethylamine / dichloromethane / 6 h / 0 - 20 °C 3: palladium diacetate; tricyclopentyl-phosphine; potassium carbonate / toluene / 8 h / 95 °C / |Glovebox View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 37 p. 13664 - 13667
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydroxide in tetrahydrofuran Suzuki coupling; 12 h; Reflux;
参考文献
Journal of Medicinal Chemistry, , vol. 55, # 14 p. 6375 - 6380
