4’-甲氧基-3-硝基-1,1’-联苯合成路线 （共 28 条）
反应条件
palladium on activated charcoal; hydrazine hydrate in ethanol T=20°C; 2 h;
参考文献
Vangala, Venu R.; Bhogala, Balakrishna R.; Dey, Archan; Desiraju, Gautam R.; Broder, Charlotte K.; Smith, Philip S.; Mondal, Raju; Howard, Judith A. K.; Wilson, Chick C.
Journal of the American Chemical Society, 2003 , vol. 125, # 47 p. 14495 - 14509
反应条件
[Pd{C6H4(CH2N(CH2Ph)2)(μ-Br)}]2; potassium carbonate in ethanol
T=60°C; Suzuki Coupling; 0.0333333 h; Microwave irradiation;
参考文献
Hajipour, Abdol Reza; Rafiee, Fatemeh
Organic Preparations and Procedures International, 2013 , vol. 45, # 6 p. 465 - 472
反应条件
sodium carbonate in water
T=100°C; Suzuki-Miyaura reaction;
参考文献
Wei, Jun-Fa; Jiao, Jiao; Feng, Jin-Juan; Lv, Jing; Zhang, Xi-Ru; Shi, Xian-Ying; Chen, Zhan-Guo
Journal of Organic Chemistry, 2009 , vol. 74, # 16 p. 6283 - 6286
反应条件
potassium phosphate; tetrabutylammomium bromide in water
T=65°C; Suzuki coupling; 0.5 h;
参考文献
Jin, Myung-Jong; Taher, Abu; Kang, Hee-Jae; Choi, Minkee; Ryoo, Ryong
Green Chemistry, 2009 , vol. 11, # 3 p. 309 - 313
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tert.-butylnitrite; trifuran-2-yl-phosphane; acetic acid in N,N-dimethyl-formamide
T=90°C; 8 h; Inert atmosphere;
参考文献
Mo, Fanyang; Qiu, Di; Jiang, Yubo; Zhang, Yan; Wang, Jianbo
Tetrahedron Letters, 2011 , vol. 52, # 4 p. 518 - 522
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=120°C; Suzuki coupling; 18 h;
参考文献
Hebel, Andre; Haag, Rainer
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9452 - 9455
反应条件
sodium carbonate; palladium fluorapatite in methanol
T=20°C; Suzuki coupling reaction; 24 h;
参考文献
Kantam, M. Lakshmi; Kumar, K. B. Shiva; Srinivas; Sreedhar
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 7 p. 1141 - 1149
反应条件
1: 1-chloro-1-(4'-methoxyphenyl)silacyclobutane With tetrabutyl ammonium fluoride in tetrahydrofuran
2: 1-iodo-3-nitro-benzene With tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran
1 h; Heating; Further stages.;
参考文献
Denmark, Scott E.; Wu, Zhicai
Organic Letters, 1999 , vol. 1, # 9 p. 1495 - 1498
反应条件
potassium phosphate; [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II) in N,N-dimethyl-formamide
T=60°C; Suzuki coupling; 24 h;
参考文献
Pourbaix, Christelle; Carreaux, Francois; Carboni, Bertrand
Organic Letters, 2001 , vol. 3, # 6 p. 803 - 805
反应条件
caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide
T=90°C; 2 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
