4’-甲氧基-3-硝基-1,1’-联苯合成路线 (共 28 条)
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane
T=20°C; Suzuki-Miyaura coupling; 8 h; Inert atmosphere;
参考文献
Nan, Guangming; Ren, Fang; Luo, Meiming
Beilstein Journal of Organic Chemistry, 2010 , vol. 6, art. no. 70
反应条件
potassium fluoride in dimethyl sulfoxide
T=105°C; 0.333333 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Huang, Dan-Feng
European Journal of Organic Chemistry, 2010 , # 3 p. 416 - 419
反应条件
sodium carbonate; polystyrene-supported N-heterocyclic carbene-Pd complex in tetrahydrofuran
Suzuki cross-coupling; 20 h; Heating;
参考文献
Zhang, Sujuan; Zeng, Xiaoming; Wei, Zhijun; Zhao, Dongbing; Kang, Tairan; Zhang, Weifeng; Yan, Mei; Luo, Meiming
Synlett, 2006 , # 12 p. 1891 - 1894
反应条件
polystyrene-supported N-heterocyclic carbene-Pd complex in ethanol
T=20°C; Suzuki-Miyaura cross-coupling; 8 h;
参考文献
Qin, Yuancheng; Wei, Wei; Luo, Meiming
Synlett, 2007 , # 15 p. 2410 - 2414
反应条件
sodium carbonate; palladium dichloride in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 0.333333 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
K3PO4*3H2O; (2-mesityl-1H-inden-3-yl)dicyclohexylphosphine; palladium diacetate; Aliquatreg; 336 in water
T=20 - 100°C; Suzuki-Miyaura Coupling; 8 h; Inert atmosphere;
参考文献
Mao, Shu-Lan; Sun, Yue; Yu, Guang-Ao; Zhao, Cui; Han, Zhi-Jun; Yuan, Jia; Zhu, Xiaolei; Yang, Qihua; Liu, Sheng-Hua
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 47 p. 9410 - 9417
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in toluene
T=40°C; Suzuki Coupling; 2 h; Sealed tube;
参考文献
Li, Yahui; Liu, Wei; Tian, Qingshan; Yang, Qing; Kuang, Chunxiang
European Journal of Organic Chemistry, 2014 , vol. 2014, # 16 p. 3307 - 3312
反应条件
polystyrene-supported N-heterocyclic carbene-Pd complex in ethanol
T=20°C; Suzuki-Miyaura cross-coupling; 12 h;
参考文献
Qin, Yuancheng; Wei, Wei; Luo, Meiming
Synlett, 2007 , # 15 p. 2410 - 2414
反应条件
palladium diacetate in tetrahydrofuran
T=20°C; Stille reaction; 1 h;
参考文献
Dughera, Stefano
Synthesis, 2006 , # 7 p. 1117 - 1122
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium methylate in ethylene glycol dimethyl ether; water
T=50°C; 5 h;
参考文献
Kang; Hong; Kim; Lee
Journal of Chemical Research - Part S, 2001 , # 7 p. 283 - 285