3-甲氧基-2-硝基苯甲酸甲酯合成路线 （共 10 条）
反应条件
potassium carbonate in DMF (N,N-dimethyl-formamide) T=20°C; 1 h;
参考文献
WO2005/113509 A1, ;
Page/Page column 121 ;
反应条件
sulfuric acid Reflux;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 15 p. 5031 - 5034
参考文献
Australian Journal of Chemistry, , vol. 29, p. 2003 - 2021
参考文献
Journal of the Chemical Society, , p. 1759,1765
反应条件
1: H2 / Pd-C 2: (i) aq. HCl, NaNO2, (ii) CuCl, aq. HCl 3: aq. NaOH View Scheme
参考文献
Cleaver,L. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 2003 - 2021
反应条件
1: H2 / Pd-C
2: (i) aq. HCl, NaNO2, (ii) CuCl, aq. HCl
View Scheme
参考文献
Cleaver,L. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 2003 - 2021
反应条件
methanol; nickel
Hydrogenation;
参考文献
JAPAN TOBACCO INC.
Patent: WO2005/113509 A1, 2005 ;
Location in patent: Page/Page column 121-122 ;
反应条件
1: H2 / Pd-C
2: (i) aq. HCl, NaNO2, (ii) CuCl, aq. HCl
3: aq. NaOH
4: aq. HBr
View Scheme
参考文献
Cleaver,L. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 2003 - 2021
反应条件
1: H2 / Pd-C
2: (i) aq. HCl, NaNO2, (ii) CuCl, aq. HCl
3: aq. NaOH
4: aq. HBr
5: NaOEt
View Scheme
参考文献
Cleaver,L. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 2003 - 2021
反应条件
1: H2 / Pd-C
2: (i) aq. HCl, NaNO2, (ii) CuCl, aq. HCl
3: aq. NaOH
4: aq. HBr
5: NaOEt
6: SOCl2 / dimethylformamide; benzene
View Scheme
参考文献
Cleaver,L. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 2003 - 2021
