7,7-二氯二环[3.2.0]庚-2-烯-6-酮合成路线 (共 14 条)
参考文献
Rey, Max; Roberts, Stanley M.; Dreiding, Andre S.; Roussel, Albert; Vanlierde, Huguette; et al.
Helvetica Chimica Acta, 1982 , vol. 65, # 3 p. 703 - 720
反应条件
1: 96 percent / NaBH4 / methanol / 21 h / Ambient temperature 2: 100 percent Chromat. / Et3N / CH2Cl2 / 7 h / Ambient temperature 3: 67 percent / NH3(liquid), Na / 3.5 h / -40 - -35 °C View Scheme
参考文献
Baldwin, John E.; Belfield, Kevin D.
Journal of Organic Chemistry, 1987 , vol. 52, # 21 p. 4772 - 4776
反应条件
1: 70 percent / Zn/Cu / acetic acid 2: baker's yeast; sucrose / H2O / 72 h / Enzymatic reaction 3: CrO3; H2SO4 4: 75 percent / MCPBA; NaHCO3 / CH2Cl2 / 25 °C View Scheme
参考文献
Fairlamb, Ian J.S.; Dickinson, Julia M.; O'Connor, Rachael; Higson, Seamus; Grieveson, Lynsey; Marin, Veronica
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 8 p. 2641 - 2656
反应条件
copper; zinc in acetic acid
参考文献
Fairlamb, Ian J.S.; Dickinson, Julia M.; O'Connor, Rachael; Higson, Seamus; Grieveson, Lynsey; Marin, Veronica
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 8 p. 2641 - 2656