2-（2-氯乙酰基）苯酚合成路线 （共 24 条）
反应条件
1: in tetrahydrofuran; toluene T=20 - 55°C; 1.5 h; Inert atmosphere; 2: With hydrogenchloride in tetrahydrofuran; toluene
参考文献
Pei, Tao; Chen, Cheng-Yi; Dimichele, Lisa; Davies, Ian W.
Organic Letters, 2010 , vol. 12, # 21 p. 4972 - 4975
反应条件
1: in tetrahydrofuran; toluene T=20 - 55°C; 1.5 h; Inert atmosphere; 2: With hydrogenchloride in tetrahydrofuran; toluene
参考文献
Pei, Tao; Chen, Cheng-Yi; Dimichele, Lisa; Davies, Ian W.
Organic Letters, 2010 , vol. 12, # 21 p. 4972 - 4975
反应条件
1: NaOAc / methanol 2: 58 percent / toluene / 24 h / Heating View Scheme
参考文献
Kozikowski, Alan P.; Gaisina, Irina N.; Yuan, Hongbin; Petukhov, Pavel A.; Blond, Sylvie Y.; Fedolak, Allison; Caldarone, Barbara; McGonigle, Paul
Journal of the American Chemical Society, 2007 , vol. 129, # 26 p. 8328 - 8332
反应条件
sodium acetate in methanol
参考文献
Kozikowski, Alan P.; Gaisina, Irina N.; Yuan, Hongbin; Petukhov, Pavel A.; Blond, Sylvie Y.; Fedolak, Allison; Caldarone, Barbara; McGonigle, Paul
Journal of the American Chemical Society, 2007 , vol. 129, # 26 p. 8328 - 8332
参考文献
Gowan et al.
Journal of the Chemical Society, 1955 , p. 862,866
参考文献
Gowan et al.
Journal of the Chemical Society, 1955 , p. 862,866
反应条件
boron trichloride; aluminium trichloride in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; 1,2-dichloro-ethane
参考文献
Shionogi and Co., Ltd.
Patent: US4551554 A1, 1985 ;
反应条件
N,N,N-trimethylbenzenemethanaminium dichloroiodate in methanol; 1,2-dichloro-ethane
10 h; Heating;
参考文献
Kajigaeshi, Shoji; Kakinami, Takaaki; Moriwaki, Masayuki; Fujisaki, Shizuo; Maeno, Kimihiro; Okamoto, Tsuyoshi
Synthesis, 1988 , # 7 p. 545 - 546
反应条件
1:
2: With aluminium trichloride
T=140°C; Further stages.;
参考文献
Kozikowski, Alan P.; Gaisina, Irina N.; Yuan, Hongbin; Petukhov, Pavel A.; Blond, Sylvie Y.; Fedolak, Allison; Caldarone, Barbara; McGonigle, Paul
Journal of the American Chemical Society, 2007 , vol. 129, # 26 p. 8328 - 8332
反应条件
in toluene
5 h; Ambient temperature;
参考文献
Sartori, Giovanni; Casnati, Giuseppe; Bigi, Franca
Journal of Organic Chemistry, 1990 , vol. 55, # 14 p. 4371 - 4377
