2-(2-氯乙酰基)苯酚合成路线 (共 24 条)
反应条件
chlorine dioxide in tetrachloromethane
T=52 - 54°C; 0.833333 h;
参考文献
Kwiecien, Halina; Jalowiczor, Jozef
Polish Journal of Chemistry, 1986 , vol. 60, # 7-12 p. 811 - 824
反应条件
beryllium(II) chloride
T=130 - 140°C;
参考文献
Bredereck et al.
Chemische Berichte, 1939 , vol. 72, p. 1414,1424
反应条件
aluminium trichloride
参考文献
Mameli
Gazzetta Chimica Italiana, 1926 , vol. 56, p. 764
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v.Auwers
Chemische Berichte, 1928 , vol. 61, p. 419
参考文献
Fucik et al.
Collection of Czechoslovak Chemical Communications, 1953 , vol. 18, p. 694,702
反应条件
aluminium trichloride; tetrachloroethane, 1,1,2,2-
参考文献
Byk-Gulden Lomberg Chem. Fabr.
Patent: DE935363 , 1954 ;
Full Text Show Details
Byk-Gulden Lomberg Chem. Fabr.
Patent: US2838570 , 1955 ;
参考文献
Fucik et al.
Collection of Czechoslovak Chemical Communications, 1953 , vol. 18, p. 694,702
反应条件
1: in tetrahydrofuran; toluene
T=20 - 55°C; 1.5 h; Inert atmosphere;
2: With hydrogenchloride in tetrahydrofuran; toluene
参考文献
Pei, Tao; Chen, Cheng-Yi; Dimichele, Lisa; Davies, Ian W.
Organic Letters, 2010 , vol. 12, # 21 p. 4972 - 4975
反应条件
1: NaI / anschliessendes Behandeln mit Dimethylamin
2: H2O; N2H4+H2O
View Scheme
参考文献
Letsinger; Collat
Journal of the American Chemical Society, 1952 , vol. 74, p. 621
反应条件
sodium hydroxide; ethanol
参考文献
Gowan et al.
Journal of the Chemical Society, 1955 , p. 862,866
反应条件
1: in tetrahydrofuran; toluene
T=-78 - -30°C; 0.5 h; Inert atmosphere;
2: With methanol in tetrahydrofuran; toluene
参考文献
Pei, Tao; Chen, Cheng-Yi; Dimichele, Lisa; Davies, Ian W.
Organic Letters, 2010 , vol. 12, # 21 p. 4972 - 4975