2,4,6-三苯基-1,3,5-三硫杂环己烷合成路线 （共 14 条）
反应条件
dichloromethane; chlorine
参考文献
Mann; Pope
Journal of the Chemical Society, 1923 , vol. 123, p. 1177
反应条件
sodium sulfide; tetrachlorosilane in acetonitrile
T=20°C; 9 h;
参考文献
Salama, Tarek A.; El-Ahl, Abdel-Aziz S.; Elmorsy, Saad S.; Khalil, Abdel-Galil M.; Ismail, Mohamed A.
Tetrahedron Letters, 2009 , vol. 50, # 43 p. 5933 - 5936
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; water
T=0°C; 0.25 h;
参考文献
Bonini, Bianca F.; Mazzanti, Germana; Zani, Paolo; Maccagnani, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1499 - 1502
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide
controlled-potential electrolysis at mercury; Further byproducts given;
参考文献
Fry, Albert J.; Ankner, Kjell; Handa, Vijay
Tetrahedron Letters, 1981 , vol. 22, # 19 p. 1791 - 1794
反应条件
in acetonitrile
T=60°C;
参考文献
Furukawa, Naomichi; Morishita, Tsuyoshi; Akasaka, Takeshi; Oae, Shigeru
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 432 - 440
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide
controlled-potential electrolysis at mercury; Further byproducts given;
参考文献
Fry, Albert J.; Ankner, Kjell; Handa, Vijay
Tetrahedron Letters, 1981 , vol. 22, # 19 p. 1791 - 1794
反应条件
1: 91 percent / 36 percent HCl / acetonitrile / 1 h / Ambient temperature
2: 26 percent / acetonitrile / 5 h / Heating
View Scheme
参考文献
Takikawa, Yuji; Shimada, Kazuaki; Makabe, Takahiro; Takizawa, Saburo
Chemistry Letters, 1983 , p. 1503 - 1506
反应条件
1: 18.6 percent / hydrogen chloride, hydrogen sulphide / diethyl ether / 0 °C
2: 70.6 percent / tetrabutylammonium fluoride / tetrahydrofuran; H2O / 0.25 h / 0 °C
View Scheme
参考文献
Bonini, Bianca F.; Mazzanti, Germana; Zani, Paolo; Maccagnani, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1499 - 1502
反应条件
acetic acid
T=60°C; 2 h;
参考文献
Furukawa, Naomichi; Morishita, Tsuyoshi; Akasaka, Takeshi; Oae, Shigeru
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 432 - 440
反应条件
sodium sulfide; ethanol
β-trithiobenzaldehyde;
参考文献
Fromm; Schmoldt
Chemische Berichte, 1907 , vol. 40, p. 2869
