3-氯-2-环戊烯-1-酮合成路线 （共 13 条）
反应条件
1: 70 percent / CH2Cl2 / 1 h / 0 °C
2: 1. n-BuLi / 1. -78 deg C, THF -> 25 deg, 2h 2. reflux, 20 min
View Scheme
参考文献
Ullrich, John W.; Chiu, Fang-Ting; Tiner-Harding, Tammy; Mariano, Patrick S.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 220 - 228
反应条件
1: 70 percent / CH2Cl2 / 1 h / 0 °C
2: 1.) THF, 60 deg C, 12h
View Scheme
参考文献
Ullrich, John W.; Chiu, Fang-Ting; Tiner-Harding, Tammy; Mariano, Patrick S.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 220 - 228
反应条件
in tetrahydrofuran
0.166667 h; Ambient temperature;
参考文献
Sakakibara; Katsumata; Watanabe; Toru; Ueno
Synthesis, 1992 , # 4 p. 377 - 379
