1: With titanium(IV) isopropylate; (1S,2S)-(-)-1,2-diphenyl-1,2-ethanediol in hexane T=20°C; 0.5 h; 2: With tert.-butylhydroperoxide in hexane T=20°C; 48 h; Further stages.;
参考文献
Capozzi, Maria Annunziata M.; Centrone, Caterina; Fracchiolla, Giuseppe; Naso, Francesco; Cardellicchio, Cosimo
European Journal of Organic Chemistry, 2011 , # 23 p. 4327 - 4334
(1S,2R,3R,4R)-2-OOH-2-(2'-furyl)-3-MeOCH2-bicyclo-heptane; titanium(IV) isopropylate in toluene T=-20°C; Title compound not separated from byproducts.;
参考文献
Lattanzi, Alessandra; Piccirillo, Sandro; Scettri, Arrigo
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 3 p. 357 - 363
1: benzyl p-bromophenyl sulphide With tert.-butyl lithium in tetrahydrofuran T=-68°C; Inert atmosphere; 2: With tri-isopropoxy-borane in tetrahydrofuran T=-68°C; Inert atmosphere; 3: methyl iodide Further stages;
