5-苯基呋喃-2(5H)-酮合成路线 （共 26 条）
反应条件
2: 89 percent / Cl2(PCy3)2Ru=CHPh / CH2Cl2 / Heating
3: 77 percent / CrO3; 3,5-dimethylpyrazole / CH2Cl2 / 1 h / -20 °C
View Scheme
参考文献
Carda, Miguel; Castillo, Encarnacion; Rodriguez, Santiago; Uriel, Santiago; Marco, J. Alberto
Synlett, 1999 , # 10 p. 1639 - 1641
反应条件
1: 89 percent / Cl2(PCy3)2Ru=CHPh / CH2Cl2 / Heating
2: 77 percent / CrO3; 3,5-dimethylpyrazole / CH2Cl2 / 1 h / -20 °C
View Scheme
参考文献
Carda, Miguel; Castillo, Encarnacion; Rodriguez, Santiago; Uriel, Santiago; Marco, J. Alberto
Synlett, 1999 , # 10 p. 1639 - 1641
反应条件
1: tetraphenylporphyrin; oxygen / CCl4 / 20 °C / Irradiation
2: iron(II) sulfate / H2O; CCl4
View Scheme
参考文献
Chen, Yu-Zhe; Wu, Li-Zhu; Peng, Ming-Li; Zhang, Dong; Zhang, Li-Ping; Tung, Chen-Ho
Tetrahedron, 2006 , vol. 62, # 46 p. 10688 - 10693
反应条件
1: Mo(CO)5*Et3N / diethyl ether / 72 h / 20 °C
2: tetraphenylporphyrin; oxygen / CCl4 / 20 °C / Irradiation
3: iron(II) sulfate / H2O; CCl4
View Scheme
参考文献
Chen, Yu-Zhe; Wu, Li-Zhu; Peng, Ming-Li; Zhang, Dong; Zhang, Li-Ping; Tung, Chen-Ho
Tetrahedron, 2006 , vol. 62, # 46 p. 10688 - 10693
反应条件
1: 1.) LDA / tetrahydrofuran
2: 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide hydrochloride, 4-N,N-dimethylaminopyridine / CH2Cl2
3: 30percent H2O2 / CH2Cl2
View Scheme
参考文献
Hanessian, Stephen; Hodges, Paul J.; Murray, Peter J.; Sahoo, Soumya P.
Journal of the Chemical Society, Chemical Communications, 1986 , # 10 p. 754 - 755
反应条件
1: 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide hydrochloride, 4-N,N-dimethylaminopyridine / CH2Cl2
2: 30percent H2O2 / CH2Cl2
View Scheme
参考文献
Hanessian, Stephen; Hodges, Paul J.; Murray, Peter J.; Sahoo, Soumya P.
Journal of the Chemical Society, Chemical Communications, 1986 , # 10 p. 754 - 755
反应条件
1: potassium borohydride, potassium hydrogen carbonate / H2O / 24 h / Ambient temperature
2: trifluoroacetic acid, trifluoroacetic anhydride / 24 h / Ambient temperature
View Scheme
参考文献
Clawson, Paul; Lunn, Patricia M.; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 159 - 162
反应条件
1: potassium borohydride, potassium hydrogen carbonate / H2O / 24 h / Ambient temperature
2: trifluoroacetic acid, trifluoroacetic anhydride / 24 h / Ambient temperature
View Scheme
参考文献
Clawson, Paul; Lunn, Patricia M.; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 159 - 162
反应条件
2: potassium borohydride, potassium hydrogen carbonate / H2O / 24 h / Ambient temperature
3: trifluoroacetic acid, trifluoroacetic anhydride / 24 h / Ambient temperature
View Scheme
参考文献
Clawson, Paul; Lunn, Patricia M.; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 159 - 162
反应条件
sulfuric acid; acetic anhydride
参考文献
Houben
Chemische Berichte, 1904 , vol. 37, p. 3981
Full Text Show Details
Erlenmeyer
Chemische Berichte, 1904 , vol. 37, p. 3127
