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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴-6-甲基吡啶
合成路线
（共 135 条）
5315-25-3
2-溴-6-甲基吡啶
→
反应条件
562086-30-0
反应条件
1: 2-bromo-6-methyl-pyridine With n-butyllithium; tributyltin chloride in tetrahydrofuran; hexane T=-78 - 20°C; 2: 4-carbomethoxy-6-methyl-2-(trifluoromethanesulfonyloxy)pyridine With triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in xylene Stille-type cross-coupling; 24 h; Heating;
参考文献
Mathieu, Julien; Marsura, Alain
Synthetic Communications, 2003 , vol. 33, # 3 p. 409 - 414
5315-25-3
2-溴-6-甲基吡啶
+
562086-28-6
→
反应条件
4411-80-7
6,6′-二甲基-2,2′-联吡啶
+
562086-30-0
反应条件
1: 2-bromo-6-methyl-pyridine With n-butyllithium; tributyltin chloride in tetrahydrofuran; hexane T=-78 - 20°C; 2: methyl 2-methyl-6-lt;(p-toluenesulfonyl)oxygt;pyridine-4-carboxylate With triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in xylene Stille-type cross-coupling; 24 h; Heating;
参考文献
Mathieu, Julien; Marsura, Alain
Synthetic Communications, 2003 , vol. 33, # 3 p. 409 - 414
5315-25-3
2-溴-6-甲基吡啶
→
反应条件
4411-80-7
6,6′-二甲基-2,2′-联吡啶
+
562086-30-0
反应条件
1: 2-bromo-6-methyl-pyridine With n-butyllithium; tributyltin chloride in tetrahydrofuran; hexane T=-78 - 20°C; 2: 4-carbomethoxy-6-methyl-2-(methanesulfonyloxy)pyridine With triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in xylene Stille-type cross-coupling; 24 h; Heating;
参考文献
Mathieu, Julien; Marsura, Alain
Synthetic Communications, 2003 , vol. 33, # 3 p. 409 - 414
5315-25-3
2-溴-6-甲基吡啶
+
1453-58-3
3-甲基吡唑
→
反应条件
526224-67-9
反应条件
rac,trans-cyclohexane-1,2-diamine; copper(l) iodide; potassium carbonate in 1,4-dioxane 24 h; RefluxInert atmosphere;
参考文献
Nasso, Isabelle; Bedel, Sebastien; Galaup, Chantal; Picard, Claude
European Journal of Inorganic Chemistry, 2008 , # 12 p. 2064 - 2074
5315-25-3
2-溴-6-甲基吡啶
→
反应条件
526224-69-1
反应条件
1: 39 percent / CuI; trans-1,2-cyclohexanediamine; K2CO3 / dioxane / Heating 2: 20 percent / NBS; AIBN / CCl4 / Heating; UV irradiation View Scheme
参考文献
Picard, Claude; Geum, Neri; Nasso, Isabelle; Mestre, Beatrice; Tisnes, Pierre; Laurent, Sophie; Muller, Robert N.; Elst, Luce Vander
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 20 p. 5309 - 5312
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