1,2-O-异亚丙基-alpha-D-木糖基-戊二醛-1,4-呋喃糖合成路线 （共 14 条）
反应条件
sodium tetrahydroborate in methanol T=20°C; 4 h;
参考文献
Zlatev, Ivan; Vasseur, Jean-Jacques; Morvan, Francois
Tetrahedron Letters, 2008 , vol. 49, # 20 p. 3288 - 3290
反应条件
1: potassium hexamethyldisilazide / tetrahydrofuran; toluene / 3 h / Ambient temperature
2: 1) 2-methyl-2-butene, borane-THF, 2) aq. NaOH, H2O2 / 1) THF, 0 deg C, 1 h, 2) RT
View Scheme
参考文献
Tsui, Hon-Chung; Paquette, Leo A.
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9968 - 9977
反应条件
n-butyllithium in tetrahydrofuran
T=-78°C; Wittig reaction; 3 h;
参考文献
Nagarapu, Lingaiah; Gaikwad, Hanmant K.; Bantu, Rajashaker; Ganesh Kumar; Pombala, Sujitha
Tetrahedron Letters, 2012 , vol. 53, # 10 p. 1287 - 1291
反应条件
potassium hexamethylsilazane in tetrahydrofuran; toluene
3 h; Ambient temperature; Yield given;
参考文献
Tsui, Hon-Chung; Paquette, Leo A.
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9968 - 9977
