苄基 2-乙酰氨基-2-脱氧-4-O-(beta-D-吡喃半乳糖基)-beta-D-吡喃葡萄糖苷合成路线 (共 6 条)
反应条件
phosphate buffer; β-D-galactosidase from Bacillus circulans in water; acetonitrile 48 h; Ambient temperaturepH 7; Yield given. Yields of byproduct given;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 6, # 10 p. 1123 - 1126
反应条件
sodium methylate in methanol 0.5 h; Ambient temperature; Yield given;
参考文献
Journal of Carbohydrate Chemistry, , vol. 17, # 4-5 p. 703 - 727
反应条件
1: 91 percent / pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 1.5 h 2: NaOMe / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 17, # 4-5 p. 703 - 727
反应条件
1: 86 percent / TMSOTf / 1,2-dichloro-ethane / 5 h / 50 °C 2: 91 percent / pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 1.5 h 3: NaOMe / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 17, # 4-5 p. 703 - 727
反应条件
1: 91 percent / pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 1.5 h 2: NaOMe / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 17, # 4-5 p. 703 - 727
反应条件
recombinant bovine milk β4 galactosyl transferase T=37°C; pH=7; aq. MES bufferEnzymatic reaction;
参考文献
Glycoconjugate Journal, , vol. 27, # 7-9 p. 673 - 684