N-(4-乙酰基苯基)甲磺酰胺合成路线 (共 12 条)
反应条件
in dichloromethane T=20 - 25°C; 1 h; Large scale;
参考文献
Zanka, Atsuhiko; Kubota, Ariyoshi; Hirabayashi, Satoshi; Nakamura, Hitoshi
Organic Process Research and Development, 1998 , vol. 2, # 2 p. 71 - 77
反应条件
potassium phosphate; copper(l) iodide; N,N-dimethylaminoacetic acid in N,N-dimethyl-formamide 48 h; Heating;
参考文献
Deng, Wei; Liu, Lei; Zhang, Chen; Liu, Min; Guo, Qing-Xiang
Tetrahedron Letters, 2005 , vol. 46, # 43 p. 7295 - 7298
反应条件
pyridine; sodium hydrogencarbonate in dichloromethane
反应条件
aluminium trichloride in 1,2-dichloro-ethane Friedel-Crafts acylation;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 7 p. 1751 - 1755
反应条件
pyridine; potassium carbonate; copper(l) chloride T=115°C; Ullmann Condensation; 6 h; Inert atmosphereLarge scale; Reagent/catalystTime;
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77
反应条件
bromine; acetic acid T=55°C; 0.25 h; regiospecific reaction;
参考文献
Zanka, Atsuhiko; Kubota, Ariyoshi; Hirabayashi, Satoshi; Nakamura, Hitoshi
Organic Process Research and Development, 1998 , vol. 2, # 2 p. 71 - 77
反应条件
bromine; acetic acid in water T=55°C; 1 h; Large scale; regiospecific reaction;
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77
反应条件
bromine; acetic acid T=55°C; 1 h; regiospecific reaction;
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77
反应条件
bromine; acetic acid T=15°C; 6 h; regiospecific reaction;
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77
反应条件
bromine; acetic acid T=15°C; 6 h; regiospecific reaction;
参考文献
Organic Process Research and Development, , vol. 2, # 2 p. 71 - 77