反应条件
1: methyl 4-O-benzoyl-2,3,6-trideoxy-α,β-L-threo-hex-2-enopyranoside With lithium aluminium tetrahydride in 1,4-dioxane
120 h; Inert atmosphereReflux;
2: tert-butyldimethylsilyl chloride With 1H-imidazole in N,N-dimethyl-formamide; toluene
Inert atmosphere; Overall yield = 91 percent; Overall yield = 29.51 g;
参考文献
Bartholomaeus, Ruben; Dommershausen, Fabian; Thiele, Markus; Karanjule, Narayan S.; Harms, Klaus; Koert, Ulrich
Chemistry - A European Journal, 2013 , vol. 19, # 23 p. 7423 - 7436
