(5-氨基-1H-吲哚-3-基)乙酸合成路线 (共 6 条)
反应条件
potassium hydroxide; hydrogen; palladium on activated charcoal in water
P=2327.2 Torr; 1.66667 h; Ambient temperature;
参考文献
Melhado, L. Lee; Pearce, Cedric J.; d'Alarcao, Marc; Leonard, Nelson J.
Phytochemistry (Elsevier), 1982 , vol. 21, # 12 p. 2879 - 2886
反应条件
1: 91 percent / Br2 / acetic acid
2: 91 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / benzene / 6 h / Heating
3: 91 percent / acetic acid / 7 h / 70 °C
5: 92 percent / conc. HCl / 6 h / Heating
6: 100 percent / hydrogen, KOH / 10percent Pd on charcoal / H2O / 1.67 h / 2327.2 Torr / Ambient temperature
View Scheme
参考文献
Melhado, L. Lee; Pearce, Cedric J.; d'Alarcao, Marc; Leonard, Nelson J.
Phytochemistry (Elsevier), 1982 , vol. 21, # 12 p. 2879 - 2886
反应条件
1: 91 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / benzene / 6 h / Heating
2: 91 percent / acetic acid / 7 h / 70 °C
4: 92 percent / conc. HCl / 6 h / Heating
5: 100 percent / hydrogen, KOH / 10percent Pd on charcoal / H2O / 1.67 h / 2327.2 Torr / Ambient temperature
View Scheme
参考文献
Melhado, L. Lee; Pearce, Cedric J.; d'Alarcao, Marc; Leonard, Nelson J.
Phytochemistry (Elsevier), 1982 , vol. 21, # 12 p. 2879 - 2886
反应条件
1: 91 percent / acetic acid / 7 h / 70 °C
3: 92 percent / conc. HCl / 6 h / Heating
4: 100 percent / hydrogen, KOH / 10percent Pd on charcoal / H2O / 1.67 h / 2327.2 Torr / Ambient temperature
View Scheme
参考文献
Melhado, L. Lee; Pearce, Cedric J.; d'Alarcao, Marc; Leonard, Nelson J.
Phytochemistry (Elsevier), 1982 , vol. 21, # 12 p. 2879 - 2886
反应条件
1: 92 percent / conc. HCl / 6 h / Heating
2: 100 percent / hydrogen, KOH / 10percent Pd on charcoal / H2O / 1.67 h / 2327.2 Torr / Ambient temperature
View Scheme
参考文献
Melhado, L. Lee; Pearce, Cedric J.; d'Alarcao, Marc; Leonard, Nelson J.
Phytochemistry (Elsevier), 1982 , vol. 21, # 12 p. 2879 - 2886
反应条件
2: 92 percent / conc. HCl / 6 h / Heating
3: 100 percent / hydrogen, KOH / 10percent Pd on charcoal / H2O / 1.67 h / 2327.2 Torr / Ambient temperature
View Scheme
参考文献
Melhado, L. Lee; Pearce, Cedric J.; d'Alarcao, Marc; Leonard, Nelson J.
Phytochemistry (Elsevier), 1982 , vol. 21, # 12 p. 2879 - 2886