in deuterated toluene byproducts: C6H5OC6H4OCH3-p; reaction of palladium complex with phosphine in toluene-d8 at 70°C;
参考文献
Stambuli, James P.; Weng, Zhiqiang; Incarvito, Christopher D.; Hartwig, John F.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 40 p. 7674 - 7677
in diethyl ether (Ar); reaction of suspn. of Pd complex (1 eqiuv., Et2O) with phosphine soln. (2 equiv., Et2O) at -30°C for 1 h, cooling (-78°C), crystn.; removal of mother liquor, drying (in vacuo);
参考文献
Journal of the American Chemical Society, , vol. 121, # 42 p. 9807 - 9823
