2，7-二氯芴-4-环氧乙烷合成路线 （共 4 条）
反应条件
1: AlCl3, aluminium chloride / dichloromethane / -5 - 0 °C 2: sodium tetrahydroborate / ethanol / 1 h / -5 - 5 °C 3: sodium methylate / 50 - 60 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 11, # 3 p. 341 - 345
反应条件
1: chlorine / acetic acid / 15 h / 35 - 45 °C 2: AlCl3, aluminium chloride / dichloromethane / -5 - 0 °C 3: sodium tetrahydroborate / ethanol / 1 h / -5 - 5 °C 4: sodium methylate / 50 - 60 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 11, # 3 p. 341 - 345
参考文献
Beutler, Ulrich; Fuenfschilling, Peter C.; Steinkemper, Andreas
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 341 - 345
反应条件
1: ethanol / 15 h / 78 °C
2: sodium hydroxide; oxygen / ethanol / 6 h / 23 - 70 °C
View Scheme
参考文献
Beutler, Ulrich; Fuenfschilling, Peter C.; Steinkemper, Andreas
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 341 - 345
