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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5324-00-5
合成路线
（共 83 条）
78579-03-0
→
反应条件
5324-00-5
反应条件
1: 78 percent / ethanol / 17 h / Heating 2: 100percent H3PO4 / 40 h / 100 °C View Scheme
参考文献
Knorr, Rudolf; Lattke, Ernst; Raepple, Edith
Chemische Berichte, 1981 , vol. 114, # 5 p. 1581 - 1591
588-59-0
二苯乙烯
→
反应条件
5324-00-5
反应条件
1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water / 19 h / 20 °C / |Inert atmosphere 2: silver tetrafluoroborate / 1,2-dichloro-ethane / 2.5 h / 65 °C / |Inert atmosphere 3: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / ethylene glycol dimethyl ether; water / 4 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Rosocha, Gregory; Batey, Robert A.
Tetrahedron, 2013 , vol. 69, # 41 p. 8758 - 8768
78579-04-1
→
反应条件
5324-00-5
+
18084-10-1
反应条件
phosphoric acid T=100°C; 40 h; Yield given. Yields of byproduct given;
参考文献
Knorr, Rudolf; Lattke, Ernst; Raepple, Edith
Chemische Berichte, 1981 , vol. 114, # 5 p. 1581 - 1591
108-86-1
溴代苯
+
1254220-92-2
→
反应条件
5324-00-5
反应条件
1: palladium catalyst / 1,4-dioxane / Reflux; Inert atmosphere; Alkaline conditions 2: sodium tetrahydridoaluminate; niobium pentachloride / 1,4-dioxane / 4 h / Inert atmosphere; Reflux View Scheme
参考文献
Fuchibe, Kohei; Atobe, Kohei; Fujita, Yukari; Mori, Keiji; Akiyama, Takahiko
Chemistry Letters, 2010 , vol. 39, # 8 p. 867 - 869
52095-44-0
→
反应条件
5324-00-5
+
18636-54-9
反应条件
1: tetrahydrofuran / -78 - 20 °C / |Inert atmosphere 2: boron trifluoride diethyl etherate / dichloromethane / 0 °C View Scheme
参考文献
Sarnpitak, Pakornwit; Trongchit, Kanokrat; Kostenko, Yulia; Sathalalai, Supaporn; Gleeson, M. Paul; Ruchirawat, Somsak; Ploypradith, Poonsakdi
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8281 - 8296
6630-33-7
邻溴苯甲醛
→
反应条件
5324-00-5
+
18636-54-9
反应条件
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 18 h / 120 °C 2: tetrahydrofuran / -78 - 20 °C / |Inert atmosphere 3: boron trifluoride diethyl etherate / dichloromethane / 0 °C View Scheme
参考文献
Sarnpitak, Pakornwit; Trongchit, Kanokrat; Kostenko, Yulia; Sathalalai, Supaporn; Gleeson, M. Paul; Ruchirawat, Somsak; Ploypradith, Poonsakdi
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8281 - 8296
292638-84-7
→
反应条件
5324-00-5
+
18636-54-9
反应条件
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 18 h / 120 °C 2: tetrahydrofuran / -78 - 20 °C / |Inert atmosphere 3: boron trifluoride diethyl etherate / dichloromethane / 0 °C View Scheme
参考文献
Sarnpitak, Pakornwit; Trongchit, Kanokrat; Kostenko, Yulia; Sathalalai, Supaporn; Gleeson, M. Paul; Ruchirawat, Somsak; Ploypradith, Poonsakdi
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8281 - 8296
108-86-1
溴代苯
+
4505-48-0
2-苯基茚
→
反应条件
5324-00-5
+
38274-35-0
反应条件
sodium amide 1) ether, 2) irradiation (BiCl3 filter), 60 min; Yield given. Multistep reaction;
参考文献
Tolbert, Laren M.; Siddiqui, Shahabuddin
Journal of Organic Chemistry, 1984 , vol. 49, # 10 p. 1744 - 1751
108-86-1
溴代苯
+
1254220-98-8
→
反应条件
5324-00-5
+
1254220-88-6
反应条件
1: palladium catalyst / 1,4-dioxane / Reflux; Inert atmosphere; Alkaline conditions 2: sodium tetrahydridoaluminate; niobium pentachloride / 1,4-dioxane / 2 h / Inert atmosphere; Reflux View Scheme
参考文献
Fuchibe, Kohei; Atobe, Kohei; Fujita, Yukari; Mori, Keiji; Akiyama, Takahiko
Chemistry Letters, 2010 , vol. 39, # 8 p. 867 - 869
108-86-1
溴代苯
+
1961-96-2
→
反应条件
5324-00-5
+
4467-88-3
+
4614-01-1
+
38274-35-0
反应条件
potassium tert-butylate 1) ether, liquid ammonia, 2) irradiation (BiCl3 filter), 30 min (90 min); Yield given. Multistep reaction. Further byproducts given;
参考文献
Tolbert, Laren M.; Siddiqui, Shahabuddin
Journal of Organic Chemistry, 1984 , vol. 49, # 10 p. 1744 - 1751
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