1,2,3,4,5,6,7,8-八氢菲合成路线 (共 80 条)
反应条件
lithium; diethylamine in tetrahydrofuran; diethyl ether T=20°C; 2 h;
参考文献
Bock, Hans; Rittmeyer, Peter
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 68, # 1-4 p. 261 - 292
反应条件
trifluorormethanesulfonic acid; PPh3 gold(I) chloro complex in 1,2-dichloro-ethane T=80°C; 18 h;
参考文献
Grise, Christiane M.; Rodrigue, Eric M.; Barriault, Louis
Tetrahedron, 2008 , vol. 64, # 5 p. 797 - 808
反应条件
hydrogen; palladium on activated charcoal in diethyl ether T=25°C; 24 h;
参考文献
Magnetic Resonance in Chemistry, , vol. 27, # 8 p. 796 - 797
反应条件
hydrogen in tetrahydrofuran T=99.99°C; P=11251.1 Torr; 2 h; AutoclaveGreen chemistry; chemoselective reaction;
参考文献
RSC Advances, , vol. 3, # 46 p. 23984 - 23988
反应条件
molybdenum(IV) disulfide; hydrogen T=390°C; P=73550.8 Torr;
参考文献
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), , vol. 11, p. 840 - 843
Chem. Zentralbl., , vol. 111, # I p. 3106
反应条件
hydrogen; tetra-n-propyl-diborane T=200°C; P=67505.4 Torr; 4 h; Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 123, # 4 p. 719 - 724
反应条件
hydrogen; polymer incarcerated palladium in ethanol T=50°C; P=53200 Torr; 24 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 69, # 8 p. 2871 - 2873
反应条件
hydrogen; tetra-n-propyl-diborane T=200°C; P=67505.4 Torr; 2 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 123, # 4 p. 719 - 724
反应条件
hydrogen; tetra-n-propyl-diborane T=200°C; P=67505.4 Torr; 10 h; Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 123, # 4 p. 719 - 724
反应条件
hydrogen; lithium aluminium tetrahydride; titanium tetrachloride in n-heptane T=200°C; P=67505.4 Torr; 10 h; other conditions: other solvent (diglyme), other times, other catalysts;; Product distribution;
参考文献
Chemische Berichte, , vol. 123, # 5 p. 983 - 987