反应条件
1: 1.) copper(I)-bromide, dimethyl sulfide / 1.) hexane, THF, 0 deg C, 15 min; 2.) THF, 0 deg C, 45 min
2: 1.) MCPBA / 1.) dichloromethane, 0 deg C, 30 min; 2.) dichloromethane, room temp. 45 min
3: 92 percent / trimethyl phosphite / toluene / 0.5 h
View Scheme
参考文献
Jones, D. Neville; Meanwell, Nicholas A.; Mirza, Sohail M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 145 - 152
